سامانه مدیریت نشریات علمی دانشگاه دامغان

سعیدی, مائده, قاضی, محمد ابراهیم, ایزدی فرد, مرتضی. (1402). سنتز و بررسی ویژگی‌های خواص ساختاری، نوری و مغناطیسی نانوکامپوزیت‌های ZnO/Fe2O3. مجله زمین شیمی ایران, 31(3), 591-602. doi: 10.61186/ijcm.31.3.591
مائده سعیدی; محمد ابراهیم قاضی; مرتضی ایزدی فرد. "سنتز و بررسی ویژگی‌های خواص ساختاری، نوری و مغناطیسی نانوکامپوزیت‌های ZnO/Fe2O3". مجله زمین شیمی ایران, 31, 3, 1402, 591-602. doi: 10.61186/ijcm.31.3.591
سعیدی, مائده, قاضی, محمد ابراهیم, ایزدی فرد, مرتضی. (1402). 'سنتز و بررسی ویژگی‌های خواص ساختاری، نوری و مغناطیسی نانوکامپوزیت‌های ZnO/Fe2O3', مجله زمین شیمی ایران, 31(3), pp. 591-602. doi: 10.61186/ijcm.31.3.591
سعیدی, مائده, قاضی, محمد ابراهیم, ایزدی فرد, مرتضی. سنتز و بررسی ویژگی‌های خواص ساختاری، نوری و مغناطیسی نانوکامپوزیت‌های ZnO/Fe2O3. مجله زمین شیمی ایران, 1402; 31(3): 591-602. doi: 10.61186/ijcm.31.3.591

سنتز و بررسی ویژگی‌های خواص ساختاری، نوری و مغناطیسی نانوکامپوزیت‌های ZnO/Fe2O3

مجله بلورشناسی و کانی شناسی ایران
مقاله 14، دوره 31، شماره 3 - شماره پیاپی 91، مهر 1402، صفحه 591-602    اصل مقاله (1.28 M)
نوع مقاله: مقاله پژوهشی
شناسه دیجیتال (DOI): 10.61186/ijcm.31.3.591
نویسندگان
مائده سعیدی؛ محمد ابراهیم قاضی* ؛ مرتضی ایزدی فرد
دانشکده فیزیک و مهندسی هسته‌ای دانشگاه صنعتی شاهرود، شاهرود، ایران
چکیده
در این پژوهش، نمونه‌های پودری ZnO، α-Fe2O3 و نانوکامپوزیت‌های ZnO/Fe2O3 با نسبت وزنی  ZnO به  Fe2O3  برابر با  (5/0: 1)، (1:1) و (1:2) به روش گرمابی تهیه و سپس ویژگی­های ساختاری­، نوری و مغناطیسی آنها بررسی شد. نتایج بررسی الگوهای پراش پرتو (XRD) نمونه­‌ها تشکیل ساختار ششگوشی اکسید روی و اکسید آهن را تائید کردند. بررسی طیف جذبی نمونه­‌های سنتز شده نشان داد که نانوکامپوزیت ZnO/Fe2O3 جذب را در ناحیه مرئی افزایش داده و از این رو مقدار گاف نواری آن نسبت به اکسید روی کاهش و نسبت به اکسید آهن افزایش می ‌یابد. تصاویر میکروسکوپ الکترونی روبشی گسیل میدانی (FESEM) نشان دادند که نانوذرات کروی Fe2O3 روی سطح نانوورقه­های ZnO قرار گرفته‌اند. نتایج مغناطیس سنج نمونه ارتعاشی (VSM) نشان دادند که ZnO خالص دارای ویژگی­ غالب دیامغناطیسی و -Fe2O3α دارای ویژگی­های فرومغناطیس نرم هستند و در نانوکامپوزیت‌های تهیه شده، با افزایش غلظت Fe2O3 مقدار مغناطش افزایش می‌یابد. به­طور کلی نتایج این تحلیل­ها نشان دادند که اندازه ذرات، ویژگی­های نوری و ویژگی­های مغناطیسی نانوکامپوزیت­های ZnO/Fe2O3 به شدت به غلظت Fe2O3-α بستگی دارند.     
کلیدواژه‌ها
روش گرمابی؛ نانوکامپوزیت ZnO/Fe2O3؛ ویژگی‌های مغناطیسی؛ ویژگی‌های نوری؛ ویژگی‌های ساختاری
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