سامانه مدیریت نشریات علمی دانشگاه دامغان

بیگمرادی, محبوبه, ایرانمنش, پروانه, سعیذنیا, سمیرا. (1403). سنتز و مشخصه‌یابی نانوفوتوکاتالیزور قابل بازیافت Ag2S/ZnS پوشش داده شده با نانوذرات Fe3O4 در تخریب رنگ متیل قرمز. مجله زمین شیمی ایران, 32(2), 379-392. doi: 10.61186/ijcm.32.2.379
محبوبه بیگمرادی; پروانه ایرانمنش; سمیرا سعیذنیا. "سنتز و مشخصه‌یابی نانوفوتوکاتالیزور قابل بازیافت Ag2S/ZnS پوشش داده شده با نانوذرات Fe3O4 در تخریب رنگ متیل قرمز". مجله زمین شیمی ایران, 32, 2, 1403, 379-392. doi: 10.61186/ijcm.32.2.379
بیگمرادی, محبوبه, ایرانمنش, پروانه, سعیذنیا, سمیرا. (1403). 'سنتز و مشخصه‌یابی نانوفوتوکاتالیزور قابل بازیافت Ag2S/ZnS پوشش داده شده با نانوذرات Fe3O4 در تخریب رنگ متیل قرمز', مجله زمین شیمی ایران, 32(2), pp. 379-392. doi: 10.61186/ijcm.32.2.379
بیگمرادی, محبوبه, ایرانمنش, پروانه, سعیذنیا, سمیرا. سنتز و مشخصه‌یابی نانوفوتوکاتالیزور قابل بازیافت Ag2S/ZnS پوشش داده شده با نانوذرات Fe3O4 در تخریب رنگ متیل قرمز. مجله زمین شیمی ایران, 1403; 32(2): 379-392. doi: 10.61186/ijcm.32.2.379

سنتز و مشخصه‌یابی نانوفوتوکاتالیزور قابل بازیافت Ag2S/ZnS پوشش داده شده با نانوذرات Fe3O4 در تخریب رنگ متیل قرمز

مجله بلورشناسی و کانی شناسی ایران
مقاله 14، دوره 32، شماره 2 - شماره پیاپی 94، مرداد 1403، صفحه 379-392    اصل مقاله (1.62 M)
نوع مقاله: مقاله پژوهشی
شناسه دیجیتال (DOI): 10.61186/ijcm.32.2.379
نویسندگان
محبوبه بیگمرادی1؛ پروانه ایرانمنش* 1؛ سمیرا سعیذنیا2
1گروه فیزیک، دانشگاه ولی‌عصر (عج) رفسنجان، رفسنجان، ایران
2گروه شیمی، دانشگاه ولی‌عصر (عج) رفسنجان، رفسنجان، ایران
چکیده
در این پژوهش، نخست نانوکامپوزیت Ag2S/ZnS به وسیله نانوذرات نقره به همراه ZnS سنتز شد سپس با بارگذاری مگنتایت روی آن،  نانوکامپوزیت مغناطیسی  ZnS/Fe3O4/ Ag2S به روش هم‌رسوبی شیمیایی تهیه گردید. برای بررسی ویژگی‌های ساختاری و ریختاری این نانوکامپوزیت‌ها از روش‌های مختلفی از جمله پراش پرتوی ایکس، طیف‌سنجی تبدیل فوریه فروسرخ (FTIR)، میکروسکوپی الکترونی عبوری، طیف­سنجی نورتابی و تخلخل‌سنجی استفاده شد. الگوی پراش پرتو x با قله‌های مشخصه ساختار مکعبیZnS ، Fe3O4 و ساختار تک میل Ag2S را تایید کرد. تحلیل FTIR به‌خوبی تشکیل پیوندهای شیمیایی مولکول‌ها را نشان داد. تخلخل نانوکامپوزیت‌ها و حضور مزوحفره­ها به روش برونر-امیت-تلر (BET) تایید شد. شدت قله نورتابی نانوکامپوزیت ZnS/Fe3O4/ Ag2Sضعیف‌تر از نانوکامپوزیت Ag2S/ZnS است که نشان دهنده کاهش موثر بازترکیب جفت الکترون-حفره و افزایش طول عمر الکترون-حفره است. این رخداد باعث افزایش عملکرد فوتوکاتالیزوری ZnS/Fe3O4/ Ag2S شد. در آخر، میزان تخریب رنگ متیل قرمز توسط این فوتوکاتالیزور‌ها بررسی شد که نانوکامپوزیت‌های Ag2S/ZnS و ZnS/Fe3O4/ Ag2S رنگ متیل قرمز را زیر تابش نور فرابنفش به ترتیب 40/76 و 80/90 درصد  در مدت زمان 75 دقیقه تخریب کردند.
کلیدواژه‌ها
نانوکامپوزیت؛ مگنتایت؛ Ag2S/ZnS؛ روش BET؛ عملکرد فوتوکاتالیزوری
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